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Pressure
We have already discussed some basics of pressure (e.g. measurement
units).
Now I would like to familiarize you with ways we mesure pressure.
The pressure within a UHV system can vary from atmospheric (when
it is vented) to 10-11 mbar and no one gauge can measure across
this wide range of pressures.
Pirani gauge (~ 100 mbar to 10-3 mbar)
Arguably the most common gauge used in surface science for measurement
at the high pressure end of the scale is the Pirani gauge. (Measurement
of pressures greater than ~ 100 mbar may be via a diaphragm gauge.
The physical principle underlying the operation of a Pirani gauge
is the pressure dependence of the thermal conductivity of a gas
below a pressure of ~ 100 mbar. (Above 100 mbar thermal conductivity
of a gas does not vary with pressure because the increase in the
number density of molecules is exactly compensated by a reduction
in the mean free path. However the smaller number density of molecules
at lower pressures means that the kinetic model picture of heat
transfer as being due to colliding molecules breaks down.)
A metal filament, usually tungsten, is held within a metal tube
connected to the vacuum system and is heated by an electric current.
The variation of the filament temperature (and thus its resistance)
with pressure is monitored using a simple Wheatstone bridge set-up.
Ion gauge (~ 10-3 mbar to 10-11 mbar)
This is the most important device in surface science for measurement
of total pressure in the medium vacuum to UHV regimes. Its operation
is based on the ionisation of molecules via a sufficiently high
energy electron beam. The ionisation rate and thus the ion current
(I+) is directly dependent on the gas pressure.
The Ion Gauge consists of three distinct parts, the filament, the
grid, and the collector. The filament is used for the production
of electrons by thermonic emission. A +ve charge on the grid attracts
the electrons away from the filament; they circulate around the
grid passing through the fine structure many times until eventually
they collide with the grid. Gas molecules inside the grid may collide
with circulating electrons. The collision can result in the gas
molecule being ionised. The collector inside the grid is -ve charged
and attracts these +ve charged ions. Likewise they are repelled
away from the +ve grid at the same time. The number of ions collected
by the collector is directly proportional to the number of molecules
inside the vacuum system. By this method, measuring the collected
ion current gives a direct reading of the pressure.
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